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@PHDTHESIS{Kaleja:236616,
author = {Kaleja, Oliver},
title = {{H}igh-precision mass spectrometry of nobelium, lawrencium
and rutherfordium isotopes and studies of long-lived isomers
with {SHIPTRAP}},
school = {Johannes-Gutenberg Universität Mainz},
type = {Dissertation},
publisher = {Johannes Gutenberg-Universität Mainz},
reportid = {GSI-2020-01337},
pages = {147 p.},
year = {2020},
note = {Dissertation, Johannes-Gutenberg Universität Mainz, 2020},
abstract = {In this work, the first successful application of the
recently developed Phase-Imaging Ion-Cyclotron Res-onance
(PI-ICR) technique in the region of the heaviest elements is
presented. For the first time, theatomic masses of several
nobelium (No,Z= 102), lawrencium (Lr,Z= 103) and
rutherfordium (Rf,Z= 104) isotopes and isomers have been
measured directly, reaching uncertainties on the order of
fewkeV/c2using the Penning-trap mass spectrometer SHIPTRAP.
These heavy radionuclides were producedin fusion-evaporation
reactions and separated from the primary beam by the
velocity filter SHIP locatedat the GSI Helmholtz Centre for
Heavy Ion Research in Darmstadt, Germany. The mass
measurementswere carried out at production rates of few ions
per second down to few ions per minute. To improvethe
overall efficiency on stopped and thermalized ions, the
recently developed cryogenic gas-stopping cellwas
implemented into the existing beam line. Its performance
with respect to purity and efficiency hasbeen characterized
and improved. The overall efficiency of SHIPTRAP is
increased by about one orderof magnitude with respect to
previous measurements on heavy ions. The atomic masses are
determinedby measuring the cyclotron frequency of the ion of
interest in the strong magnetic field of a 7 T
super-conducting magnet. The atomic masses of251No,254Lr
and257Rf were measured directly for the firsttime, reaching
high precision. The latter marks the very first direct
high-precision mass spectrometry of asuperheavy element with
a detection rate of one detected ion per day and only five
ions in total. In addi-tion, the uncertainties of the atomic
masses of254No and255,256Lr have been reduced by up to two
ordersof magnitude with respect to previous experiments at
SHIPTRAP. The precise determination of bindingenergies is
key in nuclear physics as it is a model-independent quantity
comprising all interactions that arepresent within the
atomic nucleus. This allows studying, e.g.,
quantum-mechanical shell effects, which areelementary for
the existence of (super-)heavy elements. The results of this
work are used to benchmarkatomic mass models in the vicinity
of the deformed neutron shell closure atN= 152. Furthermore,
thesemeasurements will provide additional anchor points of
very heavy odd-Nand odd-Zas well as odd-Anuclides, affecting
the masses up to darmstadtium (Z= 110). With the enhanced
mass resolving powerof up to 11 000 000, the isomeric
states251mNo,254mLr and255mLr were resolved from their
respectiveground states despite low excitation energies of
tens of keV. Their masses and the corresponding
excitationenergies were measured directly for the first
time. Up to now, only tentative level energies were
derivedfrom previousα-decay spectroscopy experiments. This
work proves the feasibility of PI-ICR in the regionof the
heaviest elements at lowest yields and particle integrals.
It paves the way to precisely study exoticsuperheavy species
with very long half-lives which becomes inevitable when
progressing towards the islandof stability.},
cin = {SHP / MSH},
cid = {I:(DE-Ds200)SHP-20080822OR107 /
I:(DE-Ds200)MSH-20150313OR333},
pnm = {612 - Cosmic Matter in the Laboratory (POF3-612) / FAIR
Phase-0 - FAIR Phase-0 Research Program (GSI-FAIR-Phase-0)},
pid = {G:(DE-HGF)POF3-612 / G:(Ds200)GSI-FAIR-Phase-0},
experiment = {EXP:(DE-Ds200)U238-20200803 / EXP:(DE-Ds200)U312-20200803},
typ = {PUB:(DE-HGF)11},
doi = {10.25358/OPENSCIENCE-5111},
url = {https://repository.gsi.de/record/236616},
}